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中药复方中熊去氧胆酸和鹅去氧胆酸的含量测定
Determination of Ursodeoxycholic Acid and Chenodeoxycholic Acidin Chinese Medicinal Compound Preparations by TLC-densitometry
【摘要】 用薄层扫描法对中药复方中熊去氧胆酸和鹅去氧胆酸测定条件进行了考察,并参照部颁熊胆粉试行标准进行了含量测定。熊去氧胆酸及鹅去氧胆酸的平均回收率分别为97.2%(RSD=1.2%)和99.3%(RSD=2.1%)。
【Abstract】 he contents of ursodeoxycholic acid (UDCA) and chenodeoxycholic acid (CDCA) in Chinese medicinal com-pound preparations have been determined by TLC-densitometry. The determination wavelength was 375nm and refe-rence wavelength was 700nm. For UDCA the linear range was 3. 0  ̄ 15. 0μg and recovery was 97. 2% (RSD =1. 2%) . and for CDCA the linear range was 4. 0 ̄20. 0μg and recovery was 99. 3% (RSD=2. 1% ).
【关键词】 熊去氧胆酸;
鹅去氧胆酸;
薄层扫描法;
【Key words】 ursodeoxycholic acid; chenodeoxycholic acid; TLC-densitometry;
【Key words】 ursodeoxycholic acid; chenodeoxycholic acid; TLC-densitometry;
- 【文献出处】 中国中药杂志 ,CHINA JOURNAL OF CHINESE MATERIA MEDICA , 编辑部邮箱 ,1995年03期
- 【分类号】R284.1
- 【被引频次】2
- 【下载频次】181