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车前根茎脂溶性化学成分的分离及结构鉴定

Isolation and structure identification of liposoluble chemical constituents in Rhizome of Plantago Asiatica L

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【作者】 李明红张永鹤朴惠善李景道郑云花

【Author】 Li Minghong;Zhang Yonghe;Piao Huishan;Li Jingdao;Zheng Yunhua(Department of Phytochemistry,Yanbian Medical College)

【机构】 延边医学院天然药物化学教研室

【摘要】 通过溶剂萃取及硅胶柱层析等分离手段,从车前根茎脂溶性成分中分离得到4种化合物。经理化性质、光谱分析及与标准品对照,鉴定了其中3种化合物,即β-谷甾醇(Ⅰ)、胡萝卜甙(Ⅱ)、乌苏酸(Ⅲ).胡萝卜甙和3,3-二环己甲基-4-(4-已基)环已基丁酸(Ⅳ)(有待于进一步鉴定)是首次从车前中分离得到的。

【Abstract】 The low-polar constituents were isolated from the rhizome of Plantago Asiatica L. by using solvent extracting method and silicagel colum chromatography etc. The structures of three compounds were identified by physicochemical property, spectral analysis and standard control as β-sitosterol(Ⅰ), daucosterine(Ⅱ)and urosolic acid(Ⅲ). The Daucosterine(Ⅱ)and 3,3-dicyclohexyl methyl-4-(4-hexyl) cyclohexyl butanoic acid(Ⅳ)that the structrue of that needs further to be identified are the first compounds isolated from this plant.

【关键词】 车前属谷甾醇类丁酸类
【Key words】 plantgositosterolsbutyric acids
  • 【文献出处】 延边医学院学报 ,Journal of Medical Science Yanbian University , 编辑部邮箱 ,1995年02期
  • 【分类号】R282.71
  • 【被引频次】5
  • 【下载频次】107
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