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微波等离子体炬原子发射光谱法测定铝铍铬钼钒锆
Determination of Al,Be,Cr,Mo,V and Zr by Microwave Plasma Torch Atomic Emission Spectrometry
【摘要】 用微波等离子体炬原子发射光谱法对Al,Be,Cr,Mo,V和Zr进行了测定,样品用超声雾化法引入。考察了实验条件的影响,建立了测定的最佳条件,测定Al,Be,Cr,Mo,V和Zr的检出限分别为5.3ng/mL,0.47ng/mL,6.0ng/mL,3.6ng/mL,5.3ng/mL和60ng/mL,线性范围为2~4个数量级,考察了一些共存物对测定的影响。
【Abstract】 The determination of Al, Be,Cr,Mo,V and Zr by microwave plasma torch atomic emis-sion spectrometry(MPT-AES)was studied.The experimental conditions were examined and opti-mized.The limits of detection for Al, Be, Cr, Mo, and Zr were 5.3ng/mL,0.47 ng/mL,6.0ng/mL,3.6 ng/mL,5.3 ng/mL and 60 ng/mL,respectively.The dynamic liear ranges were 2 to 4 or-ders of magnitude. The effects of some coexistent elements were examined.
【关键词】 难熔元素;
微波等离子体炬;
原子发射光谱法;
【Key words】 refractory element; microwave plasma torch; atomic emission spectrometry;
【Key words】 refractory element; microwave plasma torch; atomic emission spectrometry;
【基金】 国家自然科学基金
- 【文献出处】 吉林大学自然科学学报 ,ACTA SCIENTIARIUM NATURALIUM UNIVERSITATIS JILINENSIS , 编辑部邮箱 ,1995年04期
- 【分类号】O433
- 【被引频次】6
- 【下载频次】66