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六硝基六氮杂异伍兹烷的结构鉴定
STRUCTURAL IDENTIFICATION OF HEXANITROHEXAAZAISOWURTZITANE
【摘要】 用FTIR、 ̄1HNMR、 ̄(13)CNMR、MS(CI)、UV及元素分析方法鉴定了作者所合成的六硝基六氮杂异伍兹烷(CL-20)的结构,并以FTLR区分了所制得的CL-20的四种晶型(α、β、γ及ε).分析结果证明作者合成的试样的结构与文献报道的CL-20的结构式完全相符。
【Abstract】 The molecular structure of CL-20 synthesized by authors has been identi-fied by FTIR,  ̄1HNMR, ̄(13)CNMR,CIMS.UV and elemental analysis. The four poly-morphs(α,β,γ and ε)of CL-20 was prepared,and they were characterized by FTIR.The characteristic peaks of the polymorphs in the“fingerprint”region(1200~700cm ̄(-1))are in agreement with those reported in literatures. The results show that the structureof CL-20 and its four polymorphs the authors synthesized are undoubted and in high pu-rity.
【关键词】 高能量密度材料;
六硝基六氮杂异伍兹烷(CL-20);
结构分析;
【Key words】 high energy density material; hexanitrohexaazaisowurtzitane(CL-20); structural analysis.;
【Key words】 high energy density material; hexanitrohexaazaisowurtzitane(CL-20); structural analysis.;
【基金】 兵器工业总公司火炸药局资助项目
- 【文献出处】 含能材料 ,ENERGETIC MATERIALS , 编辑部邮箱 ,1995年03期
- 【分类号】TQ560.72
- 【被引频次】22
- 【下载频次】255