节点文献

环境样品中痕量邻苯二甲酸酯的分离与测定

Separation and Determination of Trace Phthalate Esters in Environmental Samples

  • 推荐 CAJ下载
  • PDF下载
  • 不支持迅雷等下载工具,请取消加速工具后下载。

【作者】 王西奎国伟林徐广通王筱梅孟平蕊

【Author】 Wang Xikui, Guo Weilin, Xu Guangtong, Wang Xiaomei, Meng Pingrui (Department of Applied Chemistry, Shandong Institute of Building Materials, Jinan 250022)

【机构】 山东建筑材料工业学院应用化学系!济南250022

【摘要】 本文研究了以小粒径(10~40μ)硅胶柱色谱分离富集、反相高效液相色谱分析测定大气颗粒物、土壤及植物样品中痕量邻苯二甲酸酯的方法.方法操作简单,回收率高,空白值低.利用该方法分析了部分环境样品中邻苯二甲酸酯含量.

【Abstract】 A method was developed for the determination of phthalate esters (PEs) in complex environmental samples, such as ambient air particulate, soil and plant samples. The main steps involved in the analysis are clean up with a column packed with fine silica gel (10 -40μ) and quantification with reversed-phase high-performance liquid chromatography e-quipped with UV detector. The overall recovery of the method for different PE is found to be more than 90%. Some analytical results of complex environmental samples were also presented.

【基金】 国家自然科学基金资助项目
  • 【文献出处】 分析化学 ,Chinese Journal of Analytieal Chemistry , 编辑部邮箱 ,1995年12期
  • 【分类号】O658
  • 【被引频次】48
  • 【下载频次】520
节点文献中: 

本文链接的文献网络图示:

本文的引文网络