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硼-姜黄素络合物的高效液相色谱研究及应用

High-performance Liquid Chromatography of Complex Derived From Boron and Curcumin and Its Application

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【作者】 胡奇志黎宏彦杨学群肖正元夏殊

【Author】 Hu Qizhi , Li Hongyan, Yang Xuequn, Xiao Zhengyuan. Xia Shu (Department of Chemistry, Xiangtan University, Xiangtan 411105)

【机构】 湘潭大学化学系湘潭大学化学系 湘潭411105湘潭411105

【摘要】 本文研究了在非水体系中硼与质子化的姜黄素形成的络合物以无水甲醇为溶剂,在C18色谱柱上用甲醇-水(80:20 V/V)作流动相(1.00mL/min)分离并检测.硼的校正曲线线性范围为 0.4~3.2μg/25mL,硼的校测限为 0.08ng.此法用于复合硼肥的分析,结果令人满意.

【Abstract】 The complex derived from boron and curcurnin was separated on a Shim-Pack CLC-ODS column(150 mm*4. 6 mm) by using a mobile phase (1. 0 mL/min) of methanol/ water (80/20, V/V), and was detected at 550 nm. The calibration graph was rectilinear in the range from 0. 4 to 3. 2 ug/25mL for boron, and the detection limit was 0. 08 ng. The method has been applied to the determination of compound boron fertilizer with satisfactory results.

  • 【文献出处】 分析化学 ,Chinese Journal of Analytieal Chemistry , 编辑部邮箱 ,1995年03期
  • 【分类号】O657.7
  • 【被引频次】8
  • 【下载频次】185
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