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六神丸中蟾毒内酯和冰片的含量测定方法
Determination of the Contents of Bufadienolide and Borneol in Liushen Pills
【摘要】 用二阶导致光谱法测定六神丸中蟾酥的主要活性成分──蟾毒内酯的含量,平均回收率为100.12%(n=6,CV%=1.44);同时用气相层析法测定冰片含量,平均回收率为97.68%(n=4,CV%=1.32)。
【Abstract】 he contents of bufadienolide and borneol in 01 and 02 Liushen Pills were determined by second-derivativespectrophotometry and gas chromatography respectively. The average recover of bufadienolide by SDS was100. 12%(n=6,RSD=1. 44%)and of borneol by GC 97. 68%(n=4, RSD=1. 32%).
【关键词】 二阶导数光谱法;
气相层析法;
蟾毒内酯;
冰片;
六神丸;
【Key words】 second-derivative spectrophotometry; gas chromatography; bufadienolide; borneol; Liushen Pills;
【Key words】 second-derivative spectrophotometry; gas chromatography; bufadienolide; borneol; Liushen Pills;
- 【文献出处】 中国中药杂志 ,CHINA JOURNAL OF CHINESE MATERIA MEDICA , 编辑部邮箱 ,1994年01期
- 【分类号】R927.2
- 【被引频次】4
- 【下载频次】117