【Abstract】 The microdisk electrode voltammetric behaviors of C60 are reported in this communication. This was accomplished by use of a mixed solvent system as Acetonotrile:Xylene = 1: 4 and a supporting electrolyte as 0.1 mol·L-1 Bu4NPF6. Au, Pt and Hg (Pt) were used as working electrode. In this new conditions, the successive six step reduction of C60 were obtained at below 15℃. It was found that the former five steps are all the single electron reversible reduction, but behaviors of the sixth steps are like EC’ processes.Several electrochemical data were determined.更多还原