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新试剂4-(5-硝基-2-吡啶偶氮)-间苯二酚分光光度法测定人发中的微量锌
Spectrophotometric determination of zinc inhuman hair by a new reagent 4-(5-nitro-2-pyridylazo)-resorcinol
【摘要】 用新试剂4-(5-硝基-2-吡啶偶氮)-间苯二酚(5-NO2-PAR)分光光度法测定了人发中微量锌。络合物的表观摩尔吸光系数为1.19×105L·mol-1·cm-1。络合比为Zn2+:5-NO2-PAR=1:2。标准加入的回收率在96%~105%之间。方法用于人发中锌含量的测定,结果令人满意。
【Abstract】 This paper reports the spectrophotometric determination of zinc in human hair by a new reagent4-(5-nitro-2-pyridylazo)-resorcinol. The apparentmolar absorptivity of the complex is 1. 19×105L·mol-1 .cm-1, and the composition is Zn2+:5-NO2-PAR=1:2. The method has been used to determine thezinc content in human hair. The standard additionalrecoveries are satisfactory.
【关键词】 锌;
分光光度法;
4-(5-硝基-2-吡啶偶氮)-间苯二酚;
【Key words】 zinc; spectrophotometry; 4-(5-nitro 2-pyridylazo)-resorcinol;
【Key words】 zinc; spectrophotometry; 4-(5-nitro 2-pyridylazo)-resorcinol;
- 【文献出处】 化学试剂 ,CHEMICAL REAGENTS , 编辑部邮箱 ,1994年01期
- 【分类号】Q581
- 【被引频次】7
- 【下载频次】91