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四正丁基溴化铵的合成
Synthesis of tetra-n-butylammonium bromide
【摘要】 以三正丁胺和1-溴代正丁烷为原料,乙腈和氯仿混合液为溶剂,在一定温度下合成了相转移剂四正丁基溴化铵。产品纯度为98.5%,产率达92.73%。
【Abstract】 The method of synthesizing tetra-n-butylammonium bromide with tri-n-butylamine and 1-bromobutane as raw-material and with acetonitrile as solvent at 90~100℃ is reported。The production rate can reach 92.7% and the purity of the product is 98.51%.
【关键词】 三正丁胺;
1-溴代正丁烷;
四正丁基溴化铵;
【Key words】 tetra-n-butylammonium bromide; tri-n-butylamine; 1-bromobutane;
【Key words】 tetra-n-butylammonium bromide; tri-n-butylamine; 1-bromobutane;
- 【文献出处】 河南医科大学学报 ,JOURNA OF HENAN MEDICAL UNIVERSITY , 编辑部邮箱 ,1994年03期
- 【分类号】TQ463
- 【被引频次】9
- 【下载频次】386