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相转移催化苯乙酸新合成方法的研究

Study about the New Synthetic Method of Phenylacetic Acid with Phase Transfer Catalyst

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【作者】 李敏谊陈亿新居绍敬

【Author】 Li Minyi;Chen Yixin;Ju Shao jing(Department of Organic Chemistry Guangdong Pharmaceutical College Guangzhou Teachers College Guangzhou 510224)

【机构】 广州师范学院

【摘要】 在相转移催化条件下氯千的羰基化反应,产物苯乙酸的产率是60%;羰基化试剂Co(co)4是在常温,常压下由Co(NO3)2制得,不须分离钝化,直接使用,是一种合成苯乙酸的新方法。本文对影响反应的因素进行了探索。

【Abstract】 This paper was about the carbonylation reaction of benzyl chloride with phase transfercatalyst.The yield of phenylacetic acid was 60%。Carbonylation regent was prpared under ordinarytemparature and presure,which was directiy utilized without separating and purifying. It was the newmethOd of Synthesizing of phenylacetic acid。 The factors of influence on the reaction were also dis。cussed

  • 【分类号】R914
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