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邻硝基苯基荧光酮流动注射分光光度法测定微量钛
Flow Injection Spectrophotometric Determina-tion of Micro amount of Titanium Using o-Nitro-phenylfluorone and Cetyltrimetbylammonium Bro-mide
【摘要】 本文研究了以邻硝基苯基荧光酮-溴化十六烷基三甲基铵为试剂的流动注射分光光度测定钛的新方法。该方法分析频率达到100次/h,线性范围为0~1.0μg/g方法重性好,用于合金钢及纯铝中钛的测定,结果满意。
【Abstract】 new method of flow injection analysis withmanifold convergence utitlizing model 72l spectropho-tometer for thedetermination of micro amount of tita-nium using o-nitrophenylfluorone andcetyltrimethylammonium bromide has been developed.The optimal reaction conditions and instru-mental parameters have been selected in detail.Themethod is simple, rapid,sensitive and selective. It hasbeen usedtodetermine micro amount of titanium inalloy steels and pure aluminium samples with repro-ducible results.
【关键词】 钛的测定;
流动注射分析;
分光光度法;
邻硝基苯基荧光酮;
【Key words】 Z Flow injecton analysis; spectropho-tometry; titanium determination; alloy steel; pure a-luminium; o-nitrophenylfluorone;
【Key words】 Z Flow injecton analysis; spectropho-tometry; titanium determination; alloy steel; pure a-luminium; o-nitrophenylfluorone;
【基金】 国家自然科学基金
- 【文献出处】 分析试验室 ,ANALYTICAL LABORATORY , 编辑部邮箱 ,1994年02期
- 【分类号】O614.411
- 【下载频次】41