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菟丝子中脂肪酸和甾醇的分析
STUDY OF FATTY ACIDS AND STEROLS IN SEED OF CUSCUTA CHINENSIS LAM.
【摘要】 采用MS和GC/MS/DS,辅以TLC,IR,熔点测定,旋光度测定等分析测试手段,对菟丝子中的脂溶性成分进行了分析研究,分离鉴定了5种甾醇和9种脂肪酸。
【Abstract】 Analytical study of fatty acids contents in seed of Cuscuta chinensis Lam.Was carried out by GC/MS/DS.Nine components were identified.The unsponifiables of lipid-soluble fraction were separated by silica gel flash chromatogaphy into six fractions.The major components of sterols were separted by silver nitrate-silica gel complex flash chromatography and identified by MS,melting point,optical rotation,GC and IR.β-sitosterol,stigmasterol,△5-avenasterol,campesterol and cholesterol were isolated and identified.
【关键词】 菟丝子;
脂肪酸;
甾醇;
色质联用;
快速层析;
【Key words】 Cuscuta chinensis; fatty acids; sterols; GC/MS,flash chromatography;
【Key words】 Cuscuta chinensis; fatty acids; sterols; GC/MS,flash chromatography;
【基金】 国家自然科学基金
- 【文献出处】 北京师范大学学报(自然科学版) ,JOURNAL OF BEIJING NORMAL UNIVERSITY , 编辑部邮箱 ,1994年04期
- 【分类号】Q949.777.1
- 【被引频次】15
- 【下载频次】253