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4-甲基-4-苯基-2-戊酮及乙酸酯的合成
【摘要】 本文介绍用苯与异丙叉丙酮在无水三氯化铝存在下通过Friedel-Crafts反应制得4-甲基-4-苯基-2-戊酮。接着用硼氢化钾还原和乙酰化反应得4-甲基-4-苯基-2-戊醇乙酸酯。总得率为56.1%。
【Abstract】 4-Methyl-4-phenyl-2-pentanone obtained by benzene with mestiyl oxide in the presence of anhydrons aluminum tricloride, which through Friedel-Crafts reaction. The ketone was treated with reduction by using potassium borohydride and acetylation to 4-methyl-4-phenyl-2-pentyl acetate. The overall yield was 56.4%.
- 【文献出处】 香料香精化妆品 ,Flavour Fragrance Cosmetics , 编辑部邮箱 ,1993年02期
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