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敌磺钠(敌克松)薄层比色分析方法研究

Study on Formulation Analysis of Fenaminosuif by TLC-Colorimetry

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【作者】 钱传范单国民卫国平邱立红南瑞然

【Author】 Qian Chuanfan Shan Guomin Wei Guoping Qiu Lihong Nan Ruiran (Dept.of Agroapplied Chemistry,Beijing Agricultural University,Beijing,100094)

【机构】 北京农业大学农业应用化学系北京农业大学农业应用化学系 北京100094北京

【摘要】 以三氯甲烷+甲醇+氨水:75+25+2为混合展开剂,将敌磺钠与样本中杂质在硅胶薄层板上分离后,用亚硫酸钠提取,在波长435 nm 测定溶液的吸光度。方法回收率在97.6%~100.8%,标准偏差为±0.50,变异系数为0.93%。

【Abstract】 A thin layer chromatography-colorimetric method for analyzing fenaminosulf has been stud- ied.Technical grade of fenaminosulf could be separated from impurities on silica gel plate developed by a mixture of chloroform/methanol/NH2·H2O solution.Fenaminosulf in silica gel was extracted by sodi- um sulfite and was detected by colorimetric method at 435 nm.The results showed that this method is suit- able for formulation analysis of finaminosulf.

【关键词】 敌磺钠薄层比色法
【Key words】 fenaminosulfTLC-colorimetric method
  • 【分类号】O656.7;S482.2
  • 【被引频次】4
  • 【下载频次】40
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