节点文献
敌磺钠(敌克松)薄层比色分析方法研究
Study on Formulation Analysis of Fenaminosuif by TLC-Colorimetry
【摘要】 以三氯甲烷+甲醇+氨水:75+25+2为混合展开剂,将敌磺钠与样本中杂质在硅胶薄层板上分离后,用亚硫酸钠提取,在波长435 nm 测定溶液的吸光度。方法回收率在97.6%~100.8%,标准偏差为±0.50,变异系数为0.93%。
【Abstract】 A thin layer chromatography-colorimetric method for analyzing fenaminosulf has been stud- ied.Technical grade of fenaminosulf could be separated from impurities on silica gel plate developed by a mixture of chloroform/methanol/NH2·H2O solution.Fenaminosulf in silica gel was extracted by sodi- um sulfite and was detected by colorimetric method at 435 nm.The results showed that this method is suit- able for formulation analysis of finaminosulf.
- 【文献出处】 北京农业大学学报 , 编辑部邮箱 ,1993年04期
- 【分类号】O656.7;S482.2
- 【被引频次】4
- 【下载频次】40