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菠萝酯的合成

SYNTHESIS OF ALLYL PHENOXYACETATE

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【作者】 王存德; 张明; 何春明; 牛岫琴; 鲁萍;

【Author】 Wang Cunde,Zhang Ming,He Chunming,Niu Xiuqin,Lu Ping (Yangzhou Institute of Technology, Postcode225001)

【机构】 扬州工学院化学教研室; 扬州工学院化学教研室 225001; 225001; 225001;

【摘要】 使用硫酸高铈固体催化剂催化苯氧乙酸和烯丙醇的酯化反应,并系统地研究了反应因素对菠萝酯收率的影响,最佳反应条件下,产物收率达80.1%~86.3%。

【Abstract】 Allyl phenoxyacetate was synthesized by phenoxyacetic acid and allyl alcohol with eerie sulfate catalyst. The effects of molar ratio,re- action time,using quantity of catalyst and solvent on the product yield from the esterifica-tion reaction have been investigated, and the optimum reaction conditions have been found.Under the optimum reaction conditions used, the yield of allyl phenoxyacetate could reach 80. 1%-86. 3%

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