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压、热敏染料中间体二苯胺衍生物的合成

SYNTHESES OF THE DERIVATIVES OF DIPHENYLAMINE USING AS INTERMEDIATES OF THE PRESSURE AND THERMAL SENSITIVE DYES

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【作者】 潘建林罗惠萍

【Author】 Pan Jianlin ,Luo Huiping (Department of Chemistry, Zhejiang University, Hangzhou 310027)

【机构】 浙江大学化学系浙江大学化学系 杭州 310027 硕士研究生杭州 310027

【摘要】 制备了2-氯-4′-羟基二苯胺,研究了原料配比和反应时间对产物得率的影响,采用两种不同的方法进行了后处理,并对该产物作了结构表征。

【Abstract】 The synthetic routes of the derivatives of diphenylamine were summarized in this paper. 2-chlro-4’-hydroxy diphenylamine was synthe-sized. The effects of mole ratios of the reac-tants and reaction time upon product yields were researched. Two different ways were carried to treat the crude products before vacuum distillation. The final product was characterized by melting point, IR, 1H-NMR.

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