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纳米粒子粒径评估及测试方法的比较

COMPARISON OF METHODS ON EVALUATION AND MEASUREMENT OF NANO-PARTICLES SIZE

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【作者】 朱静蔺锡伟郭薇贾丽萍赵向荣张晋远柳春兰叶恒强宁小光

【Author】 ZHU Jing;LIN Xiwei;GUO Wei;JIA Liping;ZHAO Xiangrong;ZHANG Jinyuan;LIU Chunlan;YE Hengqiang;NING Xiaoguang Central Iorn and Steel Research Institute, Ministry of Metallurgical Industry, Beijing Laboratory of Atomic Imaging of Solid, Institute of Metal Research, Academia Sinica, Shengyang

【机构】 洽金工业部钢铁研究总院十三室冶金工业部钢铁研究总院中国科学院金属研究所中国科学院金属研究所 教授北京(100081)

【摘要】 本文介绍了透射电镜综合分析—分散法测定纳米粒子粒径的方法,并将此法与X射线小角散射法及透射电镜暗场法测粒径进行了实验与分析的比较。认为采用X射线小角散射法与透射电镜综合分析—分散法相结合测定评估纳米粒子粒径可以以较快的速度得到准确的结果、综合的信息。

【Abstract】 Method of TEM compositive anlysis-dispersion for measuring nano-particlesize is reviewed. Comparison of methods between this and of X-ray small angle scattering aswell as of TEM in dark field was carried out by experiments and anlyses. It is believed thatcombination of X-ray small angle scattering and TEM compositive analysis-dispersionmethod is the more rapid, accurate and comprehensive way to evaluate and measure thenano-particle size.

  • 【文献出处】 金属学报 ,Acta Metallrugica Sinica , 编辑部邮箱 ,1993年01期
  • 【被引频次】9
  • 【下载频次】271
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