【摘要】 用三氯硫磷与β-羟基乙胺类化合物在四氢呋喃溶液中反应,再加入苯酚(胺),一锅反应合成了一系列2-取代苯氧(氨)基-1,3,2-氧氮磷杂环戊烷,并对其波谱性质进行了讨论.更多还原

【Abstract】 Using THF as the solvent,a series of new 2-substituted phenoxyl(anilino)-1,3,2-ox-azaphospholidine derivatives were prepared by the reaction of phosphorus sulfochloride with ami-noethanol directly and then treating with phenol or aniline in the presence of triethylamine.This is one pot reaction without the separation and purification of any intermediate and a high yield was obtained.AH of these compounds were confirmed by 1H NMR,IR,MS and elementary analysis,Their 1H NMR,and MS spectra and biological activity are discussed.更多还原