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非全消化-悬浮液进样-石墨炉原子吸收法测定人发中痕量铬
Determination of Trace Chromium in Human Hair by Non-Complete Digestion Suspension InjectionGraphite Furnace Atomic Absorption Spectrometry
【摘要】 本文提出以浓硝酸冷浸非全消化法,加OP乳化剂作稳定剂,悬浮液进样法,石墨炉原子吸收测定人发中痕量铬,取得了满意的结果。回收率为93~98%。
【Abstract】 The Conditions for determining chromium in human hair .by GFAAS.and a new method for digesting human hair have been studied. The conventional complete digestion method may result in the loss of chromium. A new method is proposed to form a suspension by soaking the hair with HNO3,adding surfactant to stabilize the colloid and then chromium content in the suspension solution is determined. The results are satisfactory. This method is simple and rapid, with recovery of 93~98% and high sensitivity.
【关键词】 发样;
非全消化;
悬浮液进样;
石墨炉原子吸收;
铬;
【Key words】 GFAAS; human hair analysis; chromium determination; sample introduction;
【Key words】 GFAAS; human hair analysis; chromium determination; sample introduction;
- 【文献出处】 分析试验室 ,Analytical Laboratory , 编辑部邮箱 ,1992年03期
- 【被引频次】6
- 【下载频次】28