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小花鬼针草叶中黄酮甙的分离与鉴定

Isolation and Identification of Flavonoid Glycosides from the Leaf of Smallflower Beggarticks(Bidens parviflora)

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【作者】 马天波; 李军林; 袁久荣;

【Author】 Ma Tian-bo, Department of Chinese Materia Medica, Shandong College of Traditional Chinese Medicine, Jinan Li Jun-lin and Yuan Jiu-rong

【机构】 山东中医学院中药系;

【摘要】 从小花鬼针草(Bidens parviflora Willd.)叶的乙醇提取物中首次分离并鉴定了4个黄酮甙类化合物,它们是紫云英甙(Astragalin,Ⅰ)、异槲皮甙(iso-Quercitin,Ⅱ)、硫磺菊甙(Sulfurein,Ⅲ)和海生菊甙(Maritimein,Ⅳ)。并采用高分辨~1HNMR和NOE技术对硫磺菊甙的芳质子归属重新作了指定。

【Abstract】 Four flavonoid glycosides were isolated from the leaf of Bidens parviflora and their structures determined by means of UV, FAB-MS, 1HNMR and 13CNMR spectroscopy. They are astragalin (Ⅰ), iso-quercitrin (Ⅱ), sulfurein (Ⅲ) and maritimein (Ⅳ). The ownership of aromatic hydrogens of sulfurein were reassigned by high resolution 1HNMR and NOE technology.

  • 【文献出处】 中草药 ,Chinese Traditional and Herbal Drugs , 编辑部邮箱 ,1991年12期
  • 【分类号】R284.2
  • 【被引频次】13
  • 【下载频次】36
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