节点文献
聚多缩乙二醇对苯二酚醚的合成及其色谱性能Ⅰ.
OLIGO(ETHYLENE GLYCOL DI(p-HYDROXYPHENYL)ETHERS)AND THEIR USE AS STATIONARY LIQUIDS FOR GAS CHROMATOGRAPHY
【摘要】 由对苯二酚与二氯甘醇反应合成了一系列聚多缩乙二醇对苯二酚醚,M=2800~4500。这些聚醚是一类高效、广谱性气相色谱固定液,可用于有机混合物的有效分离鉴定。
【Abstract】 The oligomeric ethylene glycol di-p-hydroxyphenyl ethers have been synthesized by Wil-liamson reaction of p-hydroxybenzene with dichloroethane, dichloroethylether, dichlorotrig-lycol dichlorotetraglycol and characterized by IR, UV, 1H NMR, 13C NMR. The oligomerscan be used as stationary phases in gas chromatography for separation of mixed organiccompounds: alcohols, phenols, amines, esters, and aromatic hydrocarbons.
【关键词】 聚多缩乙二醇对苯二酚醚;
合成;
气相色谱;
固定液;
【Key words】 ethylene glycol ether; oligomer; synthesis; gas chromatography; stationary phase;
【Key words】 ethylene glycol ether; oligomer; synthesis; gas chromatography; stationary phase;
- 【文献出处】 应用化学 ,Chinese Journal of Applied Chemistry , 编辑部邮箱 ,1991年06期
- 【被引频次】3
- 【下载频次】83