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薄层扫描法测定知母中知母皂甙A_Ⅲ的含量
Determination of Timosaponin A_Ⅲin Rhizoma anemarrhenae by TLC-Scanning Method
【摘要】 <正> 中药知母为百合科Liliaceae,知母属Anemarrhena Bge.植物知母Anemarrhenaasphodeloides Bge.的干燥根茎,性味苦、甘、寒,具清热泻火,生津润燥功效。知母皂甙是中药知母的有效成分之一,其中有
【Abstract】 Timosaponin AⅢ in Anemarrkena asphodeioids Bge. was determined by TLC-scanning method. 15 Pieces of samples and others came from different parts of rhizome or root. It may be separated on silica gel-CMC plates with n-butylacetic acid-water (4:1: 5, V/V, upper layer solution) and visulized with 10% phosphomolybdic acid. The amount of timosaponin AⅢ is 0.42%-2.76%. The aceuracy CV (%) is 2.48, and the average recovery is 96.8 (CV 1.28%).
【关键词】 知母;
知母皂甙;
知母皂甙A_Ⅲ;
薄层扫描法;
【Key words】 Rhizoma anemarrhenae; Anemarrhena asphodeloides Bge.; Timosaponin; Timosapoin A_Ⅲ; TLC-scanning;
【Key words】 Rhizoma anemarrhenae; Anemarrhena asphodeloides Bge.; Timosaponin; Timosapoin A_Ⅲ; TLC-scanning;
- 【文献出处】 中国药科大学学报 ,Journal of China Pharmaceutical University , 编辑部邮箱 ,1990年06期
- 【被引频次】9
- 【下载频次】92