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安钠咖注射液的薄层扫描测定法
DETERMINATION OF INJECTIO CAFFEINE ET NATRIIBENZOATIS BY TLC-SCANNER
【摘要】 采用薄层扫描法测定安钠咖注射液中咖啡因和苯甲酸钠的含量。测定方法简便、快速、结果满意。
【Abstract】 This paper reports a TLC-scanner method to determine the injectio caffeine et natriibenzoatis. The developing solventbenzene-ether-acetic acid-methnol (100:50:15:1) was used for separation of caffeine and sodium benzoate in injectio caffeine et natriibenzoatis. R_f of caffeine and sodium benzoate are 0.28, 0.74, respectively. The spots are scanned with a Shimadzu Dual-Wavelength TLC-scanner CS-930. This method was very simple, rapid and the results were quite satisfactory.
【关键词】 薄层色谱;
咖啡因/苯甲酸钠;
安钠咖注射液;
【Key words】 TLC-scan; caffeine/sodium benzoate; injectio caffeine et natriibenzoatis;
【Key words】 TLC-scan; caffeine/sodium benzoate; injectio caffeine et natriibenzoatis;
- 【文献出处】 湘潭大学自然科学学报 ,Natural Science Journal of Xiangtan University , 编辑部邮箱 ,1990年03期
- 【分类号】O658.1
- 【下载频次】11