【摘要】 研究开发的工艺过程主要包括三步:第一步,采用间歇精馏法对原料进行提纯;第二步,在三氯化铝催化剂和氯代烷烃引发剂的作用下,使原料中的甲基环戊烷异构化为环己烷。第三步,用精溜法对反应产物进行分离。通过实验确定了最佳工艺条件,并给出了工业化生产流程。更多还原

【Abstract】 The main processes include three steps.Firstly, the raw oil is purified by batch distillation method.Secondly, methyl cyclopentane in the raw oil is isomerized to cyclohexane with aluminium cloride as catalyst and chlorohydrocarbons as initiator at a temperature of 70°±5℃. Finally, the product after the reaction is separated by distillation.Through experiments, the optimal technogical conditions are determined and the industrilized production flow diagram is proposed.更多还原