【摘要】 本文以人参四逆汤中附片的有效成分为指标。用薄层色谱法作乌头类生物碱鉴别及乌头碱的限量检查。用离子对萃取—分光光度法测定乌头类生物碱含量,乌头碱的回收率为98.33%±4.72%～103.6±3.09%,加样回收率为95.09±2.09%。方法准确、重现性好。更多还原

【Abstract】 Renshen Sinitang isa formula of Chinese traditional medici-nend meteria medica. A method of thequality control of preperation was repo-rted. Both identification test of aconitealkaloids and limit test of aconitine we-re applied with TLC. Quantitative det-ermination of aconite alkaloids was ap-plied with ion pair extraction spectrop-hotometric method. The recovery of theaconitine in prepertion was 98.33±4.72%～103.6±3.09% (n=20). The internalquality of compound preperations can becontrolled with this method.更多还原