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交流示波极谱滴定法测定水中化学耗氧量
Determination of COD in water by A. C osciliographic polarographic titration
【摘要】 本文报告了用双铂片电极交流示波极谱滴定法测定水中COD的方法。研究了终点时示波极谱图的一些影响因素。实验表明,Ag(Ⅰ),Cd(Ⅱ),CO(Ⅱ),Ni(Ⅱ),Zn(Ⅱ),Mn(Ⅱ),PO43-,NO3-,Cl-,Br-,均不影响终点示波图形观察,本法也适合于在高浓度强酸中直接滴定。
【Abstract】 This paper describes determination of COD in water by A. C oscillographic polarographic titration on two identical Pt electrodes. The factors are discussed affecting oscillographic polarographic figure near end point. The experiment results show that Ag( Ⅰ ) , Hg( Ⅱ ) , Cw( Ⅱ ) , Co(Ⅱ) , Mn(Ⅱ) , Mi(Ⅱ) , Zn(Ⅱ) , Cd( Ⅱ ) , PO43- NO3- Cl- Br- I-do not that end pointobserved. This method may by used in the determination of COD in water with a large amount of strong acid.
【关键词】 交流示波极谱;
化学耗氧量;
【Key words】 A. C oscillographic polarographic titration. COD chemical oxygen demanded;
【Key words】 A. C oscillographic polarographic titration. COD chemical oxygen demanded;
- 【文献出处】 怀化师专学报(自然科学) , 编辑部邮箱 ,1990年01期
- 【被引频次】1
- 【下载频次】25