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糙叶败酱挥发油成分的分离与鉴定

Isolation and identification of the constituents of volatile oil from the Chinese drug Cao Ye Bai Jiang,rhizome and root of Patrinia scabra Bunge

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【作者】 田珍陈战松楼之岑梁伟升庞吉海

【Author】 Tian Zhen CHEN Zhan-song LOU Zhi-cen (Department of Pharmacognosy,Beijing Medical University,Beijing)LI ANG Wei-sheng PANG Ji-hai (Department of Spectral Analysis,Beijing Medical University,Beijing)

【机构】 北京医科大学生药教研室北京医科大学波谱分析室

【摘要】 糙叶败酱 Patrinia scabra Bge.的根与根茎的挥发油前人报告证明有镇静作用。作者对该挥发油采用了气-质联用方法,并结合快速柱层分离和经红外光谱及氢核磁共振光谱鉴定了其中5种成分,主成分为石竹烯,另有α-古芸烯、β-古芸烯,α-律草烯及正十六烷。这些成分均为首次自该植物中分出并鉴定的。

【Abstract】 Five components were identified from thevolatile oil separated by stemdistillationof the dried rhizome and root of Patrinia seabra Bunge(family Valerianaceae)byGC-MS,and three of them were coufirm-ed by I R and NMR after further isolationby means of flash column chromatography.The main component was found to be cary-ophyllene,and the others were α-humulene,α-,β-gurjunene and hexadecane.The prese-nce of these compounds in the volatile oilof this plant has not yet been reported pre-viously.

  • 【文献出处】 中国药学杂志 ,Chinese Pharmaceutical Journal , 编辑部邮箱 ,1989年02期
  • 【被引频次】4
  • 【下载频次】38
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