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毛细管气相色谱法测定牡丹皮中丹皮酚的含量

DETERMINATION OF PAEONOL CONTAINED IN THE TRADITIONAL CHINESE DRUG MOUTAN CORTEX(PAEONOL SUFFRUTICOSA) BY CAPILLARY GAS CHROMATOGRAPHY

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【作者】 段玲汪丽霞相秉仁安登魁

【Author】 Duan Ling, Wang Lixia, Xiang Bingren and An Dengkui Department of Pharmaceutical Analysis

【机构】 中国药科大学药物分析研究室中国药科大学药物分析研究室

【摘要】 本文应用正交设计一单纯形优化方法对牡丹皮中丹皮酚进行毛细管气相色谱分离优化,建立了相应的定量分析方法。在所测浓度范围内,峰面积与被测物浓度的线性关系良好。本法较为简便,重现性好,回收率为99.28%,变异系数为2.6%(n=15)。

【Abstract】 Determination of paeonol contained in the traditional Chinese drug moutan cortex by capillary GC was presented. Calibration graph linear in the detected range and recovery was 99.28% (CV% 2.6, n=5). The paeonol contents in P.suffruticosa obtained from different territories were detected and were agreeable with those obtained by direct-steam distillation-UV method and HPLC method. The result showed that the proposed method was simple and effective.

  • 【文献出处】 中国药科大学学报 ,Journal of China Pharmaceutical University , 编辑部邮箱 ,1989年05期
  • 【被引频次】7
  • 【下载频次】180
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