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用国产树脂富集提取海水中荻氏剂的GC法

ACCUMULATION OF DIELDRIN FROM SEA WATER ONTO THE DOMESTIC RESIN AND ITS GC DETERMINATION

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【作者】 孙淑媛蔡水源郑邦定

【Author】 Sun Shuyuan, Cai Shuiyuan and Zheng Bangding(Third Institute of Oceanography, SOA, Xiamen)

【机构】 国家海洋局第三海洋研究所国家海洋局第三海洋研究所 厦门厦门厦门

【摘要】 本文介绍了海水中ng/L含量获氏剂的GC分析方法:即树脂柱的预处理和样品中获氏剂的富集、提取黄铜矿;样品提取液的脱水、净化、分离和GC测定;获氏剂的确证试验;方法的试验结果。

【Abstract】 The feasibity of gas chromatographic determination of dieldrin in sea water was examined by the following processes: dieldrin in sea water was accumulated onto a domestic 1300 (1) resin and the extract was purified and separated in a combined SiO2-Al2O3-Na2SO4 column, and then concentrated with nitrogen gas and determined by gas chromatography.Good recoveries were reached by this method with a mean recovery of 86%, and a standard deviation of 5%. The results show that this method is acceptable to determining dieldrin of ng/L level in sea water.

  • 【文献出处】 台湾海峡 ,Journal of Oceanography In Taiwan Strait , 编辑部邮箱 ,1989年02期
  • 【被引频次】1
  • 【下载频次】19
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