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气相色谱法快速测定蚊香及蚊香原料中丙烯菊酯
Rapid Determination of Allethrin in Mosquito Coil and Its Raw Material by Gas Chromatography
【摘要】 <正> 丙烯菊酯是蚊香的活性组分。关于蚊香中丙烯菊酯的测定报道甚少。文献中[1]采用电子俘获检测器检测,线性关系差,检测器易污染。文献[2]中采用振摇提取,操作繁琐。本法采用甲醇超声提取,气相色谱分离,FID检测操作简单,快速,准确。
【Abstract】 By means of supersonic extraction technique and gas chromatography with a column of 0.28% OV-17 (?)3% OV-210/Chromosorb W HP, 80-l00mesh,φ3.0mm×2.1m, a simple, rapid, accurate analytical method for alletnrin in mosquito coil and its raw material has been proposed. The results obtained by this method are satisfactory with a recoveries ranging from 92.7% to 99.0% and coefficients of variation from 1.64%to 3.31%.
- 【文献出处】 色谱 ,Chinese Journal of Chromatography , 编辑部邮箱 ,1989年06期
- 【被引频次】1
- 【下载频次】36