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土壤中痕量钼的催化光度测定法
SPECTROPHOTOMETRIC DETERMINATION OF ULTRA TRACE AMOUNTS OF MOLYBDENUM IN SOIL BY A NEW CATALYTIC REACTION
【摘要】 本文研究了钼(Ⅳ)在 HCl—KCl 缓冲液介质中催化过氧化氢氧化对氨基乙酰苯胺和β—萘酚的显色反应。并拟定了催化分光光度测定土壤中痕量钼的新方法,本方法的灵敏度为8×10-10g/ml,测定范围0~1.0μg/25ml,本法已用于土壤中痕量钼的测定。
【Abstract】 In this paper,the Mo(Ⅵ)catalytic effect on the colour reaction,inwhich the mixture reductant of β-naphthylaminc and P-Aminoa clortanilide isoxidized by H2O2 in a buffer solution HCl-KCl,has been examined in detail.Optimum condition for determining Mo(Ⅵ)had been established.The sen-sitivity of this method was presented as 8×10-10g/ml,The range of determ-ination was 0~1.0μg/25ml.This method has been used in determining the tr-ace amounts of Mo(Ⅵ)in soil.
- 【文献出处】 江西农业大学学报 ,Acta Agriculturae Universitis Jiangxiensis , 编辑部邮箱 ,1989年04期
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