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用PIXE方法分析人发中微量元素时数据质量问题剖析

AN ELEMENTARY ANALYSIS ON THE DATA QUALITY OF TRACE ELEMENT DETERMINATION IN HAIR BY PIXE

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【作者】 沙因刘平生张润华

【Author】 SHA YIN;LIU PINGSHENG;ZHANG RUNHUA Institute of High Energy Physics, Academia Sinica, Beijing

【机构】 中国科学院高能物理研究所中国科学院高能物理研究所 北京北京北京

【摘要】 <正> 头发是人体排泄微量元素的器官之一,头发中微量元素的含量间接地反映人体中微量元素的含量。头发中微量元素的含量能反映一定时间内人体微量元素含量的情况。它可以作为环境条件和人体功能的“指示器”,给出环境污染和人体健康与疾病的信息。而发样又

【Abstract】 The data quality of trace element determination in human hair by PIXE isfairly improved, when three measures are adopted: 1, The sample is thinhomogeneous and smooth, especially the sample thicrness is controlled about 0.1-0.2 mg/cm; 2, Acomputer program with mutli-function for the analysis ofcomplex X-ray spectra (PAXMF) is used. Tbe PAXMF program not only gives outthe net areas of characteristic peaks but also can calculate the concentration ofelements in the sample, can subtract the interferences contributed by impuritiesin "blank sample" and can provide practical detection limits for the user; 3,System error is corrected by means of determination of trace elements in humanhair standard material. 16 trace elements are analysed in human hair sample by PIXE as anintercomprarision, the values of 7 elements (Ca, Ti, Mn, Fe, Ni, Zn, Pb) are ingood agreement with the recommended values.

【关键词】 质子激发X荧光分析数据质量
【Key words】 PIXEData quality
  • 【文献出处】 原子能科学技术 ,Atomic Energy Science and Technology , 编辑部邮箱 ,1988年03期
  • 【被引频次】4
  • 【下载频次】27
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