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活性氮与丙烯反应的研究
Study on the Reaction of Active Nitrogen With Propene
【摘要】 作者使活性氮与丙烯进行反应,得到与前人不同的产物,如:C5H7N3、C6H9N3、C7H11N3等含奇数氮的化合物。所用活性氮系纯氮气流在工频电场中辉光放电获得;反应在常温下及压力在0.26—2.6kPa(20~200mmHg)间进行;产物用液氮冷凝收集。文中介绍了反应装置、主要设备规格及详细实验操作并报告了分析鉴定条件和结果。
【Abstract】 Active nitrogen has been made to react with propene. The products obtained are different from what they were before,for instance, C5H7N3, C6H9N3, C7H11N3, C7H11N3 etc. odd nitrogen compounds. The active nitrogen used is obtained from glow discharge, of pure nitrogen current in electric field of industrial frequency. The reaction is made at ordinary temperature and the pressure, of 0.26—2.6kPa 20—200mmHg. The products are condensed by liquid nitrogen and are collected. The reaction devices and the size of the main equipment are introduced. The detail of experiment operation and the analytical consults are reported.
- 【文献出处】 沈阳化工学院学报 ,Journal of Shenyang Institute of Chemical Technology , 编辑部邮箱 ,1988年01期
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