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凝胶渗透色谱法对双带火药中的硝化纤维素、硝化甘油和中定剂的分离测定
Separation and Determination of Nitrocellulose(NC), Nitroglycerine (NG) and Centralite (C2) in Double-Base Powder Stripe by Gel Permeation Chroma-tography
【摘要】 <正> 将双带火药直接溶解于四氢呋喃溶剂中,使呈一均匀高分子和低分子的混合溶液,再将此溶液引入到凝胶色谱体系中,使高、低分子得到分离。采用内标法,对分离后的双带火药的主要成分硝化纤维素(NC),硝化甘油(NG)和中定剂(C2)进行定量测定。
【Abstract】 NC, NG and C2 in double-base powder stripe have been separated and quantitatively determined by GpC using a 7.8× 300mm column comprised of two stainless steel tubes in series, packed with Ultrastyragel 50nm and 10nm, aad tetrahydrofuran as mobile phase with a R401 differential refraction detector- Polystyrene was used as the internal stanhard. The method is simple, rapid and accurate.
- 【文献出处】 色谱 ,Chinese Journal of Chromatography , 编辑部邮箱 ,1988年02期
- 【被引频次】1
- 【下载频次】81