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亚钛还原法测定重氮氯化锌复盐的含量

THE DETERMINATION OF CONTENT OF DIAZONIUM SALT IN TITANOMETRY

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【作者】 蒋昌翎;

【Author】 Jiang Changling Department of Chemistry

【机构】 湖南师范大学化学系;

【摘要】 本文阐述了用改进的亚钛还原法,测定本单位试制的一种新的重氮感光试剂——3-甲基-4-吡咯啶基苯重氮氯化锌复盐的含量,结果为98.78%。

【Abstract】 In this paper,the convenient condition ofanalys is is expounded,when we usetitanometry to determine the content of diazonium salt in semifinished product:wetake in the order of operation that the sample is put in the titanium trichloridesolution slowly;the quantity of titanium trichloride is in excess of 200% or so;the time of reaction is 20 minute.Using this method,the content of 3-methyl-4-pyrrolidinyl benzene diazonium zine chloride,a new diazo light sensitive agent,is determined accuratly.It is 98.78%.

  • 【文献出处】 湖南师范大学自然科学学报 ,Journal of Natural Science of Hunan Normal University , 编辑部邮箱 ,1988年03期
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