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环境标样茶叶、茶树叶的制备及均匀性测定

PREPARATION AND HOMOGENEITY-ASSESSMENT OF TEA AND TEA LEAVES STANDARD REFERENCE MATERIALS

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【作者】 韩恒斌; 刘淑琴; 张淑贞; 张永兰; 吴涤尘; 金龙珠; 倪哲明; 粟德永;

【Author】 Han Hengbin Liu, Suqin Zhang Suzhen Zhang YenglanWu Dichen Jin Longzhu Li Deyong Ni Zheming (Research Center for Eco-Environmental Sciences, Academia Sinica)

【机构】 中国科学院生态环境研究中心; 中国科学院西北植物所;

【摘要】 本文报导环境标准物质茶叶、茶树叶的制备和均匀度的评价。茶叶和茶树叶采集于陕西黄家山茶园,样品经过空气干燥、研磨、过60目筛、混匀和装瓶等步骤处理,然后用钴60照射灭菌(2Mrd)。照射后的样品随机抽样采用中子活化和原子吸收分析方法,测定其中,Zn,Cu,Fe,Mn,Ca,K,Al,S和P等元素的含量,测定结果用F和t检验法处理,结果表明样品的均匀度达到标准物质的要求。

【Abstract】 The preparation and homogeneity assessment of tea and tea leaves standard reference materials are reported.The tea and tea leaves for tea reference materials were collected from tea garden (Huangjia Shan, Shanxi). The collected materials were air dried, ground sieved to pass a 60 mesh screen, blended and bottled. Then all bottles were sterilized by Co-60 radiation (2M rad).The homogeneity-assessment was tested by determining the contents of some elements (Zn. Cu, Fe, Mn, Ca. K. Al. S. and P) by X-ray floures-cence analysis and atomic absorption spectrometry By applying F and t testes it was indicated that the prepared tea and tea tree leaves satisfies the homogeneity criteria for a reference material.

【基金】 国家自然科学基金
  • 【文献出处】 环境化学 ,Environmental Chemistry , 编辑部邮箱 ,1988年06期
  • 【被引频次】2
  • 【下载频次】28
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