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废水中安乐康及某些有机残留物的HPLC分析

DETERMINATION OF CLOPIDOL AND OTHER ORGANIC RESIDUES IN WASTE WATER BY HPLC

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【作者】 练鸿振; 张文彬; 王连生; 田笠卿;

【Author】 Lian Hongzhen Zhang Weribin Wang Liansheng Tian Liqing(Center of Materials Analysis, Nanjing University)

【机构】 南京大学现代分析中心; 南京大学环境科学系; 南京大学现代分析中心;

【摘要】 本文研究了用高效液相色谱法(HPLC)测定生产安乐康的废水中安乐康及某些有机残留物含量的方法。废水经0.45μm滤膜过滤后,注入反相ODS柱,用甲醇和水作流动相进行梯度洗脱,在280nm检测,有机残留物被清晰地分开,方法简便、快速。本法测出的废水中有机残留物的含量,与水样的COD值及其外观具有一致性。另外,我们用此法比较了不同处理方法对该废水进行处理的效果,发现用5%活性炭吸附和电解法结合处理效果最佳。

【Abstract】 A method for the determination of clopidol and other organic residues in wastewater by high performance liquid chromatography has been developed. The wastewater was filtered through a 0.45μm milipore membrane filter,then injected into a reversed-phase ODS column and measured at 280nm. The organic residues could be eluted and separated clearly when methanol-weter was used as the mobile phace. This method is Simple, easy and rapid. The amount of organic residues detected are found to be consistent with the app-earence and COD values of the wastewater. The method was used to com-pare the effectiveness of several different water treatment processes. It was, found that 5 % active carbon absorption combined with electrolysis is the most efficient.

  • 【文献出处】 环境化学 ,Environmental Chemistry , 编辑部邮箱 ,1988年05期
  • 【被引频次】2
  • 【下载频次】18
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