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Er（PMAP）₃·2H₂O的合成及其晶体结构和分子结构

The Synthesis and Crystal, Molecular Structure of Er（PMAP）₃·2H₂O

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【Author】 Chen Botao, Ren Liping (Department of Chemistry, Bering Normal University. Beijing)Luo Baosheng, Zhan Liaorong (The Analysis and Testing Centre, Wuhan Univesity, Wuhan)

【机构】北京师范大学化学系；北京师范大学化学系；武汉大学分析测试中心；武汉大学分析测试中心北京农业大学；

【摘要】 Er（PMAP）₉·2H₂O（PMAP=1-苯基-3-甲基-4-乙酰吡咯啉酮-5）属单斜晶系。空间群为P2₁/c,晶胞参数α=17,582（4）,b=12.346（2）,c=18.236（3）,β=102.8（2）°,Z=4,R=0.06298。更多还原

【Abstract】 Er(PMAP)3·2H2O crystal belongs to monoclinic system. α=17.582 (4) A, b= 12.346(2) A,c = 18.236(3) A, β=102.8(2)°. Space group P21/c, Z = 4. The diffraction data(Mo, Kα) were collected with type CAD4(Holland) fpurcircle diffractomer. The structure was determined by heavy atom method and refined by least square program, R = 0.06298更多还原