【摘要】 本文设计了双β-乙基碳酸锗倍半氧化物(以下简弥Ge-132)的氧化还原定量分析方法。先用湿法破坏Ce-132后以次亚磷酸纳将四价锗还原成二价锗,然后用碘液滴定二价锗的方法间接测定其含量。更多还原

【Abstract】 A method used for determining the content of bis-beta-ethylcarbonium acid germanium sesqui oxide （Ge-132） is described in this paper. Ge⁴⁺ was reduced to Ge²⁺ by sodium hypophosphite after Ge-132 had been destroyed by wet procedure, and then Ge²⁺ was titrated with standard solution of iodine, thereupon, amount of Ge-132 to be calculated. The report describes the condition of the destruction and oxido-redu ction. Recovery varied from 99.78 to 100.0±0.1042%.更多还原