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激光晶体BeAl2O4:Cr3+生长缺陷的电镜观察

TEM OBSERVATION OF GROWTH DEFECTS IN LASER CRYSTAL BeAl2O4:Cr3+

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【作者】 郭行安陈梅玲李乃仁秦清海黄明芳李宗全秦勇

【Author】 Guo Xingan Chen Meiling Li Nairen Qin Qinghai Huang Mingfang(Anhui Institute of Optics and Fine Mechanics, Academia Sinica)Li Zongguan Qin Yong(Institute of Solid State Physics, Academia Sinica)

【机构】 中国科学院安徽光学精密机械研究所中国科学院固体物理研究所中国科学院固体物理研究所

【摘要】 本文报道提拉法c轴生长紫翠宝石(BeAl2O4·Cr3+)激光晶体中生长缺陷的电镜观察结果。晶体生长中出现的云层区中存在大量的气泡,包裹物、位错、小角晶界等缺陷。胞状结构的胞壁附近存在大量的包裹物。相邻胞体之间存在取向差。在垂直于晶体生长方向的(001)面上观察到可滑移位错。对这些缺陷的形成原因进行了初步的分析。

【Abstract】 This paper presents TEM observation results of growth defects in Alexandrite laser crystals BeAl2O4:Cr2+ grown on c-axis by Czochralski method. There is a large number of defects in regions of cloud striations including bubbles, inclusions, dislocations, lowangle grain boundaries.It is found that there is a large number of inclusions in cell walls of cellular stucture and an orientation difference between two neighbouring cells is also existed. Gliding dislocations in direction perpendicular to c-axis are also observed. In addition causes of the defects have been briefly discussed in the paper.

  • 【文献出处】 硅酸盐学报 ,Journal of The Chinese Ceramic Society , 编辑部邮箱 ,1987年04期
  • 【被引频次】1
  • 【下载频次】39
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