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A3钢基体磁控溅射离子镀铝膜相组成的研究

AN INVESTIGATION ON THE PHASES OF THE MAGNETRON SPUTTERING ION PLATING ALUMINUM FILM ON THE A3 STEEL SUBSTRATE

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【作者】 王玉魁薛春朱英臣余广华王斐杰陈宝清

【Author】 Wang Yu-Kui Xue Chun Zhu Ying-chen Y Guanghua Wang Fei-jic Chen Bao-qing (Ion Plating Research Division, Dalian Institute of Technlogy)

【机构】 大连工学院离子镀研究所

【摘要】 本文应用X射线衍射分析和电子衍射分析研究了A3钢基体磁控溅射离子镀铝膜的相组成。结果表明,膜的相组成主要是基板负偏压决定的。当基板负偏压低于300V时磁控溅射离子镀铝膜是单质铝膜;当基板负偏压为500V时镀膜中心出现了Al13Fe4相;随着基板负偏压增加,膜中相继出现了Al5Fe2、AlFe和AlFe3等含铁量高的Fe-Al化合物相。

【Abstract】 The phases of the magnetron sputtering ion plating aluminum film on the A3 steel substrate have been examined by means of X-ray diffraction analysis and TEM. The results showed that the phases of the film are mainly dependent on the negative bi(?)s of the substrate. When the negative biases are lower than 300 volts, the film is purely made of the element of the target, aluminum. When the negative bias of 500 volts is applied to the substrate, only one phase, Al13Fe4, is found in the film. With the increase of the voltage of negative bias, the phases rich in Fe, Al5Fe2, AlFe and AlFe3would be appeared successively in the film.

  • 【文献出处】 金属热处理学报 ,Transactions of Metal Heat Treatment , 编辑部邮箱 ,1986年02期
  • 【被引频次】3
  • 【下载频次】66
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