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NiTi合金中应力诱导无公度相/公度相可逆转变的研究

A Study of Stress-induced Reversible I/C Transition in NiTi Alloy

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【作者】 张进修林光明黄元士林旭江庆华杨海波邵自昌洪伟卿

【Author】 Zhang Jinxiu Lin Guangmin Huang Yunshi Lin Xu Jiang Qinghua (Department of Physics,Zhongshan University)Yang Haibo Shao Zichang Hong Weiqing (Institute of Iron and Steel Research of Shanghai)

【机构】 中山大学物理学系上海钢铁研究所上海钢铁研究所

【摘要】 在超弹性NiTi 合金室温加载、卸载的应力循环过程中,在同一样试上同时测量了应变、模量、电阻率以及内耗随应力的变化,研究了应力循环周数对上述四个参数的影响.结果表明:在增加应力至应变为4%后卸载时,试样表现了完整的超弹性,即应力卸载至零时,应变完全回复到零,这说明全部应变都是由应力诱导的可逆相变提供的.在增加应力时,电阻率单调上升并变平,模量出现极小值而内耗出现极大值;减小应力时,上述过程滞后地出现.当试验温度远高于母相转变为无公度I 相的温度T_I 时,以及试验温度低于M_f 点时,上述超弹性以及变载过程中出现的电阻、内耗及模量的变化特征均消失.将上述结果和NiTi含金在变温过程中电阻、内耗及模量的变化规律进行对比,以及对应力诱导循循环前后试样的X 光衍射分析结果均表明,上述超弹性是由于NiTi 合金中应力诱导的无公度相I/公度相C间的可逆转变所提供的.由于应力诱导I/C 转变的可逆性,因此这一转变将对NiTi 合金的双程形状记忆效应产生一定的影响.研究了应力循环周数对可逆I/C 转变的影响.

【Abstract】 The interal friction Q-1,modulus f2,resistance R and the strain (?) of superelast-icity Ni51Ti49 alloy in the process of stress-induced incommensurate/commensu-rate(I/C)transition was measured as a function of stress σ at room temperatu-re.This NiTi samples posses superelasticity up to about 4% of strain which isprovided completely with strain of stress-induced reversible I/C transition strainand this strain reverses zero when the stress is unloading to zero.A minimum in the f2-σ curves and a peak in the Q-1-σ curves were observedfor the first time during the loading process and a reversible change appeareshysteretily in the unloading process.The compareson of these phenomenons withathermal transition of I/C in NiTi and the results of X-ray diffraction of stre-ss-cycled TiNi samples show that the superelasticity of NiTi alloy is provided com-pletely with strain of stress-induced reversible I/C transition.The mobility ofI/C phase interface was discussed.

  • 【文献出处】 中山大学学报(自然科学版) ,Acta Scientiarum Naturalium Universitatis Sunyatseni , 编辑部邮箱 ,1985年03期
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