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60Co-γ射线辐照猪肉辐解产物的气相色谱测定

Gas Chtomatographic Measurement of the Radiolytic Products of the Irridiated Pork

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【作者】 周应才; 汪秀英; 徐培书; 袁必槐;

【Author】 Zhou Ying-cai, Wau.q Xiu-ying, Xu Pei-shu & YuanBi-huai,Institute of Applied Nuclear Technology, Chengdu, Sichuan Proutnce.

【机构】 四川省原子核应用技术研究所; 四川省原子核应用技术研究所 成都; 成都; 成都;

【摘要】 <正> 在用射线辐照灭菌保藏食品中,辐解产物对食品风味有一定影响。弄清它们的组成不仅对工艺参数(如辐照的剂量、温度、气氛)的选择提供某些依据,而且对食品卫生安全性的说明和辐解机理的推测也有一定的意义。 三十多年来,国外对这一课题的不断深入研究已经积累了大量的资料。仅就辐照肉类来说,就鉴定出了100余种挥发性组分,主要是脂肪辐解产生的烷烯烃,少量的炔烃和羰基化物以及蛋白质辐解所产生的硫化物和芳香烃等。

【Abstract】 The radiolytic products of a pork were isolated, analyzed and identified by the techniques of vacuum distillation, GC and GC-MS. The higher-boiling compounds in the fat were collected by cold-finger and the lower-boiling compounds were recovered on a short precolumn packed with alumina. The volaliles of the lean pork were collected on a short column packed with TCEP/Chromosorb. Some conditions in the experimental were studied. 49 compounds were identified. The compounds include the hydorcarbons and sulphides eic.

  • 【文献出处】 色谱 ,Chinese Journal of Chromatography , 编辑部邮箱 ,1985年03期
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