节点文献
N-(α,β-双取代-4-氯桂皮酰基)-另丁胺类化合物的NMR及构型研究
THE STUDY OF NMR ON THE N-(α,β-DISUBSTITUTED-4-CHLOROCINNAMYL)-SEC.-BUTYLAMINE DERIVATIVES
【摘要】 本文报道了N-(α,β—双取代-4-氯桂皮酰基—另丁胺类化合物的1H NMR及13C NMR的研究。通过比较该类化合物分子酰胺基中氢及碳的化学位移指定了各化合物的构型。采用NMR方法判定的构型为X光衍射结果所证实。
【Abstract】 In the present paper the 1H NMR and 13C NMR spectral data of N-(disu-bstituted - 4 - chloro-cinnamyl) -sec. -butylamine compounds were reportedCompared the chemical shifts of hydrogen and carbon in the amide groups ofthe compounds, the configurations of the compounds were assigned.The configurations assigned according to NMR were proved by the results of X-ray diffraction of the crystals of the compounds.
【基金】 中国科学院科学基金
- 【文献出处】 波谱学杂志 ,Chinese Journal of Magnetic Resonance , 编辑部邮箱 ,1985年01期
- 【被引频次】7
- 【下载频次】20