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闪蒸-毛细管气相色谱-质谱法分析中草药的挥发性成分

Analysis Of Volatile Constituents Of Chinese Medicinal Herbs by Flash Distillation-Capillary Gas Chromatography-Mass Spectrometry

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【作者】 陈耀祖; 李兆林; 薛敦渊; 韩辉; 杨玉成;

【Author】 Chen Yaozu, Li Zhaolin, Xue Dunyuan, Han Hui and Yang Yuchcng (Department of Chemistry, Lanzhou University, Lanzhou)

【机构】 兰州大学化学系; 兰州化工研究院; 青海高原心脏病研究所;

【摘要】 本文采用闪蒸-毛细管气相色谱-质谱法对姜黄、茅苍术、小茴香、肉桂的主要挥发性组分进行了分析,其结果与常规分析相符,对中草药闪蒸分析的条件进行了探讨,实验结果证明,闪蒸分析法是研究中草药挥发性成分的一种简便、快速、有效的微量分析方法。

【Abstract】 In present paper, the principal volatilc constituents of Chinese medicinal herbs, Curcuma longa L., A. lancea(Thunb.)DC.,Foeniculum vulgare Mill. And cinna-momun cassia presl have been analyzed by means of flash distillation/capillary gas chromatography/mass spectrometry. The results obtained were similar to that of conventional steam distillation-extration method. But this new technique possesses such advantages: rapidity, simple manipulation, micro quantity of plant sample used and the exclusion of interference from impurities in the extrating solvents. It proves to be a promising tool for analysis of volatile constituents of natural products. The optimum condition of flash distillation has also been studied.

  • 【文献出处】 高等学校化学学报 ,Chemical Research In Chinese Universities , 编辑部邮箱 ,1985年12期
  • 【被引频次】31
  • 【下载频次】111
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