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三（α-萘荒酸）合铬（Ⅲ）Cr(α-C10H7CS2)3.1/2CH2Cl2的合成与晶体结构
The Synthesis and Crystal Structure of Tri(α-Dithionaphthoato) Chromium, Cr(α-C10H7CS2)3·1/2 CH2C12
【摘要】 合成了铬的六配位络合物Cr(α-C10H7CS2)3·1/2CH2Cl2。用x射线单晶衍射法测定了晶体结构。晶体属单斜晶系,空间群C2h6-C 2/C。晶胞参数:a=23.020（4）（?）,b=15.032（4）（?）,c=19.468（5）（?）,β=112.91（1）°,Z=8。最小二乘修正引出最终偏差因子R=0.063,R∞=0.050。
【Abstract】 The title compound has been synthesized and the crystal structure of this compound has been determined by the single-crystal X-ray diffraction method.The crystal belongs to monoclinic system, space group C26h-C2/c with unit cell parameters. a=23.020(4)A, b = 15.032(4)A, c = 19.468(5)A, β = 112.91(1)°, V = 6205 (2)A3, Z = 8. The structure was refined to R = 0.063, R, = 0.050.
- 【文献出处】 北京大学学报(自然科学版) ,Acta Scicentiarum Naturalum Universitis Pekinesis , 编辑部邮箱 ,1985年06期
- 【被引频次】1
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