节点文献
{Mo[S2CN（C2H5）2]4}+{MoCl6}-的合成及其晶体结构与分子结构
Synthesis, Crystal Structure and Molecular Structure of {Mo[S2CN(C3H5)2]4} + {MoCl6}-
【摘要】 我们合成了化合物{Mo[S2CN（C2H5）2]4}+{MoCl6}-,确定了其所属晶系、空间群及晶胞参数,并确定了重原子与其它全部非氢原子坐标等.
【Abstract】 We have Synthesized a compound, for which molecular formula is {Mo[S2CN(C2H5)2]4}+{MoCl6}-, and determined its crystal structure by X-ray diffraction method. It is monoclinic, space group P21/a, with cell dimensions a = 14.716(6) A, b = 16.012(6) A, c= 17.108(9)A, β = 102.63 (4)° and Z=4. The structure was solved by Patter son method and refined by using the Least-squares method to final consistence factors R= 0.0908, Rw= 0.0761.
- 【文献出处】 高等学校化学学报 ,Chemical Research In Chinese Universities , 编辑部邮箱 ,1984年04期
- 【被引频次】5
- 【下载频次】22