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当归化学成份分析研究——毛细管气相色谱-质谱法鉴定当归根挥发油成份
ANALYSIS OF THE INGREDIENTS OF ANGELICA SINENSIS——ANALYSIS OF THE INGREDIENTS OF ESSENTIAL OIL BY CAPILLARY COLUMN GC/MS
【摘要】 <正> 当归具有活血化瘀、镇静、解痉等作用.分析其化学成份对研究其药理作用具有极重要的意义.自1924年开始,即有这方面的研究报导.我们从生药当归(Angelicasinensis(Oliv.)Diels,甘肃岷县收购的)根的挥发油中分离鉴定出 37种成份,其中32种为首次自岷县当归中发现.挥发油自当归根碎片中水蒸汽蒸馏获得,得率0.4%,
【Abstract】 In present work, the chemical ingredients of the essential oil of roots of Angelica Sinensis (Oliv.) Diels have been analyzed by capillary column GC/MS. 19, 12 and 6 compounds have been identified from the neutral, phenolic and acidic fractions respectively.Among them 32 constituents have not been found in this species before. By high resolution mass spectrometry and metastable ion scanning technique, the fragmentation pattern of ligustilide, a principal constituent of the essential oil, has been studied.
- 【文献出处】 高等学校化学学报 ,Chemical Research In Chinese Universities , 编辑部邮箱 ,1984年01期
- 【被引频次】97
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