节点文献
气相色谱无阀切换流程和“组合”检测器的研究
Investigation of Valveless Switching Technique and Multifunction (Four in One) Detector for Gas Chromatography Zhou Liangmo Zhu Daoqian Wang Qinghai Wang Guanghua Ye Fen Li Yulan Lu Peizhang (Dalian Institute of Chemical Physics,Academia Sinica)
【作者】
周良模;
朱道乾;
王清海;
王光华;
叶芬;
李玉兰;
卢佩章;
【Author】
By using two dimension valveless column switching system solvent-cut, heart-cut, back-flush and transfer mode operation can be performed to offer better resolution, shorter analy-tical time as well as protecting the main analytical column. Results are given in packed-packed column, packed-capillary column and capillary-capillary column combination.In addition, a four in one multifunction detector which has FID, ECD FPD and NPDfunctions was developed for identification and determination of complex mixtures. It can beused as a single detector and also a multi-responses detector simultaneously as well. Bothpacked and capillary column have been combined with this new detector for monitoring somespecial compounds in a complex mixture. A new intelligent gas chromatograph with columnswitching system and multifunction detector is now in developing in our institute.
【机构】
中国科学院大连化学物理研究所;
中国科学院大连化学物理研究所;
【摘要】 <正> 气相色谱作为一种快速、高效、高灵敏度的分析方法,其应用范围越来越广。目前多通道(multichannel)、多维(multi-dimension)、多种检测器、多功能和全盘自动化的仪器,以及随着微处理机化的迅猛发展,使气相色谱进入了向“智能化”发展的新阶段,为了实现“智能化”色谱的操作控制自动化、条件方法最佳化以及谱图分析计算机化的要求。必须使色谱分析或色谱仪的“硬件”——柱系统成更多还原
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【文献出处】
分析化学
,Chinese Journal of Analytical Chemistry
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编辑部邮箱
,1984年05期
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